Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside

Base Information

Chemical Name:Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside
CAS No.:159501-64-1
Molecular Formula:C₂₄H₂₉O₁₀P
Molecular Weight:508.462
Hs Code.:

Methyl 3,4-di-O-acetyl-2-O-<bis(benzyloxy)phosphoryl>-β-D-xylopyranoside

Synonyms:Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside

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Technology Process of Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside

There total 2 articles about Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 612-05-5
methyl-β-D-xylopyranoside

: 159501-64-1
Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / molecular sieves 4-Angstroem / acetonitrile / 55 h / 30 °C / lipase PS

2: 1.) 1H-tetrazole, 2.) RuCl₃*3H₂O, sodium periodate / 1.) CH₂Cl₂, CH₃CN, r.t., 2 h, 2.) H₂O, r.t., 1 h

With 1H-tetrazole; ruthenium trichloride; sodium periodate; 4 A molecular sieve; In acetonitrile;
DOI:10.1021/jo00102a029

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 77217-82-4,63629-70-9
methyl 3,4-di-O-acetyl-β-D-xylopyranoside

: 159501-64-1
Methyl 3,4-di-O-acetyl-2-O--β-D-xylopyranoside

Guidance literature:: With 1H-tetrazole; ruthenium trichloride; sodium periodate; Yield given. Multistep reaction; 1.) CH₂Cl₂, CH₃CN, r.t., 2 h, 2.) H₂O, r.t., 1 h;
DOI:10.1021/jo00102a029