(1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate

Base Information

Chemical Name:(1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate
CAS No.:1263875-91-7
Molecular Formula:C₄₇H₇₄O₅Si
Molecular Weight:747.187
Hs Code.:

Synonyms:(1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate

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Technology Process of (1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate

There total 1 articles about (1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1263876-07-8
(2R)-1-((4R,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)-4-penten-2-ol

: 814-68-6,25189-84-8
acryloyl chloride

: 1263875-91-7
(1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0030-1258253

Reference yield: 75.0%

: 1263875-91-7
(1R)-1-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-3-butenyl acrylate

: 1263876-08-9
(6R)-6-[((4S,6S)-6-[(3S)-3-([(tert-butyl)diphenylsilyl]oxy)heptadecyl]-2,2-dimethyl-1,3-dioxan-4-yl)methyl]-5,6-dihydro-2H-2-pyranone

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 40 ℃; for 3h;
DOI:10.1055/s-0030-1258253