methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

Base Information

Chemical Name:methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate
CAS No.:1208307-81-6
Molecular Formula:C₃₉H₃₉NO₇S
Molecular Weight:665.807
Hs Code.:

Synonyms:methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

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Chemical Property of methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

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Technology Process of methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

There total 6 articles about methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52508-44-8
2-benzyloxy-3-hydroxymethyl-1-methoxybenzene

: 175214-62-7
C₂₄H₂₅NO₅S

: 1208307-81-6
methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2009.10.126 DOI:10.1016/j.bmcl.2009.10.115

Reference yield:

: 34805-17-9
methyl 2S-amino-3-(4-benzyloxyphenyl)propionate hydrochloride

: 1208307-81-6
methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 4 h / 0 - 25 °C / Inert atmosphere

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

With triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 2.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2013.10.013

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1208307-81-6
methyl (S)-2-(N-(2-(benzyloxy)-3-methoxybenzyl)-4-methylphenylsulfonamido)-3-(4-(benzyloxy)phenyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 4 h / 0 - 25 °C / Inert atmosphere

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

With triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 2.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2013.10.013