methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

Base Information

Chemical Name:methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside
CAS No.:497234-46-5
Molecular Formula:C₁₉H₂₉O₈P
Molecular Weight:416.408
Hs Code.:

Synonyms:methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

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Chemical Property of methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

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Technology Process of methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

There total 11 articles about methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: Oxalic acid 2-benzyloxy-1-(dimethoxy-phosphoryl)-1-((3aR,4S,6S,6aS)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-ethyl ester methyl ester

: 497234-46-5
methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

: 497234-45-4
methyl (5R)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-α-D-mannofuranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃;
DOI:10.1016/S0008-6215(03)00235-0

Reference yield: 16.0%

: Oxalic acid (R)-2-benzyloxy-1-(dimethoxy-phosphoryl)-1-((3aR,4S,6S,6aS)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-ethyl ester methyl ester

: 497234-46-5
methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

: 497234-45-4
methyl (5R)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-α-D-mannofuranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 2h;
DOI:10.1002/1522-2675(200209)85:9<2608::AID-HLCA2608>3.0.CO;2-F

Reference yield: 15.0%

: Oxalic acid (S)-2-benzyloxy-1-(dimethoxy-phosphoryl)-1-((3aR,4S,6S,6aS)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-ethyl ester methyl ester

: 497234-46-5
methyl (5S)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-β-L-gulofuranoside

: 497234-45-4
methyl (5R)-6-O-benzyl-5-deoxy-5-dimethoxyphosphinyl-2,3-O-isopropylidene-α-D-mannofuranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 2h;
DOI:10.1002/1522-2675(200209)85:9<2608::AID-HLCA2608>3.0.CO;2-F