4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

Base Information

Chemical Name:4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid
CAS No.:1357186-05-0
Molecular Formula:C₁₇H₁₆ClN₃O₂
Molecular Weight:329.786
Hs Code.:

Synonyms:4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

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Chemical Property of 4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

Chemical Property:

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Technology Process of 4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

There total 4 articles about 4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1357186-04-9
4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carbonitrile

: 1357186-05-0
4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

Guidance literature:: 4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carbonitrile; With water; sodium hydroxide; for 8h; Reflux;

With hydrogenchloride; In water; ethyl acetate; pH=2;

Reference yield:

: 1357186-03-8
4-chloro-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carbonitrile

: 1357186-05-0
4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane / 1 h / 150 °C / Microwave irradiation

2.1: sodium hydroxide; water / 8 h / Reflux

2.2: pH 2

With hydrogenchloride; water; sodium hydroxide; In 1,4-dioxane;

Reference yield:

: 202823-67-4
3,6-dichloro-4,5-diazatricyclo[6.2.2.2,7]dodeca-2⁽⁷⁾,3,5-triene

: 1357186-05-0
4-[(3-chlorophenyl)amino]-5,6,7,8-tetrahydro-5,8-ethanophthalazine-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen iodide; sodium iodide / 0.67 h / 120 °C / Microwave irradiation

2.1: acetonitrile / 0.67 h / 160 °C / Microwave irradiation

3.1: hydrogenchloride / 1,4-dioxane / 1 h / 150 °C / Microwave irradiation

4.1: sodium hydroxide; water / 8 h / Reflux

4.2: pH 2

With hydrogenchloride; water; hydrogen iodide; sodium iodide; sodium hydroxide; In 1,4-dioxane; acetonitrile;