Technology Process of C20H26O4
There total 3 articles about C20H26O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trimethylsilyl iodide;
In
acetonitrile;
for 24h;
Heating;
DOI:10.1021/jm00147a031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) Mg / 1.) ether, reflux, 0.5 h, 2.) ether, reflux, 2 h
2: 39 percent / TiCl3, LiAlH4 / 1,2-dimethoxy-ethane / 16 h / Heating
3: 31 percent / trimethylsilyl iodide / acetonitrile / 24 h / Heating
With
lithium aluminium tetrahydride; titanium(III) chloride; trimethylsilyl iodide; magnesium;
In
1,2-dimethoxyethane; acetonitrile;
DOI:10.1021/jm00147a031
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 39 percent / TiCl3, LiAlH4 / 1,2-dimethoxy-ethane / 16 h / Heating
2: 31 percent / trimethylsilyl iodide / acetonitrile / 24 h / Heating
With
lithium aluminium tetrahydride; titanium(III) chloride; trimethylsilyl iodide;
In
1,2-dimethoxyethane; acetonitrile;
DOI:10.1021/jm00147a031