Technology Process of C34H49NO7Si
There total 6 articles about C34H49NO7Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
toluene;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1039/c2jm30357d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammomium bromide; potassium carbonate; sodium iodide / acetone / 6 h / Reflux
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C / Darkness; Inert atmosphere
3: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 4 h / 20 °C / Inert atmosphere
With
dmap; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; tetrabutylammomium bromide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium iodide;
In
dichloromethane; acetone; toluene;
DOI:10.1039/c2jm30357d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C / Darkness; Inert atmosphere
2: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene / 4 h / 20 °C / Inert atmosphere
With
dmap; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; toluene;
DOI:10.1039/c2jm30357d
