(3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

Base Information

Chemical Name:(3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate
CAS No.:1202794-83-9
Molecular Formula:C₂₂H₃₀N₂O₇
Molecular Weight:434.489
Hs Code.:

Synonyms:(3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

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Chemical Property of (3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

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Technology Process of (3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

There total 1 articles about (3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1222844-21-4
C₁₈H₂₄N₂O₅

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1202794-83-9
(3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

: 1202794-82-8
(3S,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1021/ol902438f

Reference yield: 74.0%

: 1202794-83-9
(3R,4S,5R)-methyl 5-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-3-hydroxy-2-methylenehept-6-enoate

: 1202794-69-1
(3R,4S,5R)-methyl 3-(benzyloxycarbonylamino)-4-(tert-butoxycarbonylamino)-5-hydroxycyclopent-1-enecarboxylate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol902438f