Technology Process of C17H24N2O5S2
There total 4 articles about C17H24N2O5S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
dichloromethane;
Inert atmosphere;
DOI:10.1021/jm400457y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol / 2.5 h / Reflux; Inert atmosphere
2: caesium carbonate / N,N-dimethyl-formamide / Inert atmosphere
3: diisobutylaluminium hydride / dichloromethane / Inert atmosphere
With
diisobutylaluminium hydride; caesium carbonate;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm400457y
- Guidance literature:
-
Multi-step reaction with 4 steps
1: amino sulfide; pyridine; triethylamine / water / 18 h / 60 °C / Inert atmosphere
2: ethanol / 2.5 h / Reflux; Inert atmosphere
3: caesium carbonate / N,N-dimethyl-formamide / Inert atmosphere
4: diisobutylaluminium hydride / dichloromethane / Inert atmosphere
With
pyridine; amino sulfide; diisobutylaluminium hydride; caesium carbonate; triethylamine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm400457y