2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

Base Information

Chemical Name:2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone
CAS No.:1279712-23-0
Molecular Formula:C₂₂H₂₈O₁₁S
Molecular Weight:500.524
Hs Code.:

Synonyms:2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

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Chemical Property of 2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

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Technology Process of 2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

There total 4 articles about 2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 74590-54-8
2-phenylethyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-mannopyranoside

: 1279712-23-0
2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.01.012

Reference yield:

: 74590-54-8
2-phenylethyl 2,3,4,6-tetra-O-acetyl-1-thio-α-D-mannopyranoside

: 1279712-23-0
2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

: C₂₂H₂₈O₁₀S

Guidance literature:: With water; In acetone; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1007/s00706-013-0964-0

Reference yield:

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-Mannose pentaacetate

: 1279712-23-0
2-phenylethyl 2,3,4,6-tetra-O-acetyl-α-d-mannopyranosyl sulfone

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 24.25 h / 0 - 20 °C / Inert atmosphere; Cooling with ice

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/j.ejmech.2011.01.012