3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Base Information

Chemical Name:3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole
CAS No.:1021326-91-9
Molecular Formula:C₂₃H₂₄N₄O₉S₂
Molecular Weight:564.597
Hs Code.:

Synonyms:3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

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Chemical Property of 3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

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Technology Process of 3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

There total 4 articles about 3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1021326-90-8
5-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-4-amino-2,4-dihydro-[1,2,4]triazole-3-thione

: 65-85-0,8013-63-6
benzoic acid

: 1021326-91-9
3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Guidance literature:: With trichlorophosphate; for 8h; Heating;
DOI:10.1080/15257770701296978

Reference yield: 37.0%

: 13228-96-1
6-phenyl-s-triazolo<3,4-b><1,3,4>thiadiazole-2H-3-thione

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1021326-91-9
3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

: 1021326-96-4
2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-6-phenyl-2H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-3-thione

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide;
DOI:10.1080/15257770701296978

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 1021326-91-9
3-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylthio)-6-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / phosphoric trichloride / 8 h / Heating

2: 37 percent / triethylamine / dimethylformamide

With triethylamine; trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1080/15257770701296978