N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

Base Information

Chemical Name:N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine
CAS No.:1310682-65-5
Molecular Formula:C₁₉H₁₇Cl₄N₅O
Molecular Weight:473.189
Hs Code.:

Synonyms:N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

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Chemical Property of N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

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Technology Process of N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

There total 5 articles about N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1310682-76-8
1-(3,4-dichlorophenyl)-3-isopropyl-2-methylisothiourea

: 2-amino-3-(3,4-dichlorophenyl)imidazolin-4-one

: 1310682-65-5
N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

Guidance literature:: With potassium carbonate; In propan-1-ol; N,N-dimethyl-formamide; at 110 ℃; for 48h; Inert atmosphere;

Reference yield: 70.0%

: 1310682-76-8
1-(3,4-dichlorophenyl)-3-isopropyl-2-methylisothiourea

: 1310682-82-6
2-amino-1-(3,4-dichlorophenyl)-1,5-dihydroimidazol-4-one

: 1310682-65-5
N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

Guidance literature:: With potassium carbonate; In propan-1-ol; N,N-dimethyl-formamide; Inert atmosphere; Heating;
DOI:10.1021/jm200111g

Reference yield:

: 74188-45-7
1-(3,4-dichlorophenyl)-3-isopropyl thiourea

: 1310682-65-5
N-(3,4-dichlorophenyl)-N'-[1-(3,4-dichlorophenyl)-4-oxo-4,5-dihydro-1H-imidazol-2-yl]-N''-isopropylguanidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetone / 60 °C / Inert atmosphere

1.2: 25 °C / Alkaline conditions; Inert atmosphere

2.1: potassium carbonate / propan-1-ol; N,N-dimethyl-formamide / Inert atmosphere; Heating

With potassium carbonate; In propan-1-ol; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm200111g