Technology Process of C19H19N3O2
There total 6 articles about C19H19N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 25 °C
2: caesium carbonate; dimethylaminoacetic acid; copper(l) iodide / dimethyl sulfoxide / 0.5 h / 130 °C / Inert atmosphere
3: trifluoroacetic acid / dichloromethane / 2 h
With
copper(l) iodide; dimethylaminoacetic acid; caesium carbonate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 1.5 h / 25 °C
2: dimethylsulfide borane complex / tetrahydrofuran / 3 h / Reflux
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 25 °C
4: caesium carbonate; dimethylaminoacetic acid; copper(l) iodide / dimethyl sulfoxide / 0.5 h / 130 °C / Inert atmosphere
5: trifluoroacetic acid / dichloromethane / 2 h
With
copper(l) iodide; dimethylaminoacetic acid; dimethylsulfide borane complex; caesium carbonate; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;