C₂₅H₃₅NO₅S

Base Information

Chemical Name:C₂₅H₃₅NO₅S
CAS No.:1365392-18-2
Molecular Formula:C₂₅H₃₅NO₅S
Molecular Weight:461.623
Hs Code.:

C<sub>25</sub>H<sub>35</sub>NO<sub>5</sub>S

Synonyms:C₂₅H₃₅NO₅S

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Chemical Property of C₂₅H₃₅NO₅S

Chemical Property:

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Technology Process of C₂₅H₃₅NO₅S

There total 11 articles about C₂₅H₃₅NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₃NO₅S

: 1365392-18-2
C₂₅H₃₅NO₅S

Guidance literature:: With borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; toluene; at 20 ℃; for 1.08333h; stereoselective reaction; Inert atmosphere;
DOI:10.1248/cpb.59.1523

Reference yield:

: 492471-45-1
9-oxo-13-hydroxy-14,15,16,17,18,19,20-heptanor-5-thia-8-azaprostanoic acid methyl ester

: 1365392-18-2
C₂₅H₃₅NO₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / ethyl acetate / 0.33 h / 0 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

3.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.08 h / 20 °C / Inert atmosphere

With borane-THF; sulfur trioxide pyridine complex; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; ethyl acetate; toluene; mineral oil; 1.1: Parikh-Doering oxidation / 2.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1248/cpb.59.1523

Reference yield:

: C₁₂H₁₄O₃

: 1365392-18-2
C₂₅H₃₅NO₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / acetonitrile / 1 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / hexane; toluene / 1 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 1.5 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 °C / Inert atmosphere

4.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran; toluene / 1.08 h / 20 °C / Inert atmosphere

With n-butyllithium; borane-THF; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; hexane; toluene; acetonitrile; mineral oil; 3.2: Horner-Wadsworth-Emmons olefination;
DOI:10.1248/cpb.59.1523