Technology Process of (E)-1-(4-chlorophenyl)-1H-1,2,3-triazole-4-carbaldehyde oxime
There total 4 articles about (E)-1-(4-chlorophenyl)-1H-1,2,3-triazole-4-carbaldehyde oxime which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C
1.2: 1 h / 0 - 5 °C
2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C
3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C
4.1: hydroxylamine hydrochloride; sulfuric acid / ethanol / 24 h / 20 °C
With
hydrogenchloride; copper(ll) sulfate pentahydrate; sulfuric acid; hydroxylamine hydrochloride; sodium L-ascorbate; sodium nitrite; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
ethanol; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2013.12.039
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C
2: hydroxylamine hydrochloride; sulfuric acid / ethanol / 24 h / 20 °C
With
sulfuric acid; hydroxylamine hydrochloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
ethanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2013.12.039