aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:859838-48-5
Molecular Formula:C₆₃H₆₉NO₁₁
Molecular Weight:1016.24
Hs Code.:

Synonyms:aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 5 articles about aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 859838-47-4
2-azidoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-α-D-glucopyranoside

: 859838-48-5
aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With ammonium hydroxide; ethanol; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1016/j.jorganchem.2005.03.020

Reference yield:

: 100-44-7
benzyl chloride

: 859838-48-5
aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / NaOH / dimethylsulfoxide / 18 h / 18 °C

2: aq. NH₃; Ph₃P; aq. EtOH / tetrahydrofuran / 48 h / 20 °C

With ammonium hydroxide; sodium hydroxide; ethanol; triphenylphosphine; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/j.jorganchem.2005.03.020

Reference yield:

: 3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4
1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose

: 859838-48-5
aminoethyl 2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: sodium methylate / methanol

3: sodium hydride / N,N-dimethyl-formamide

4: Lindlar's catalyst; hydrogen

With Lindlar's catalyst; boron trifluoride diethyl etherate; hydrogen; sodium methylate; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/psc.2774