C₂₁H₂₂NP

Base Information

• Chemical Name: C₂₁H₂₂NP
• CAS No.: 202977-11-5
• Molecular Formula: C₂₁H₂₂NP
• Molecular Weight: 319.386
• Mol file: 202977-11-5.mol

Synonyms:C₂₁H₂₂NP

Chemical Property of C₂₁H₂₂NP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₂₂NP

There total 4 articles about C₂₁H₂₂NP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

Methylphenylamino-phenylchlorphosphin (20685-01-2) + (2,6-dimethylphenyl)magnesium bromide (21450-64-6) → C21H22NP (202977-11-5)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/a706428d

Reference yield:

Dichlorophenylphosphine (644-97-3) → C21H22NP (202977-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran; hexane / 1.) r.t., 45 min, 2.) r.t., 2 h

2: 89 percent / tetrahydrofuran / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane;

DOI:10.1039/a706428d

Reference yield:

N-methylaniline (100-61-8) → C21H22NP (202977-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / tetrahydrofuran; hexane / 1.) r.t., 45 min, 2.) r.t., 2 h

2: 89 percent / tetrahydrofuran / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane;

DOI:10.1039/a706428d

upstream raw materials:

Methylphenylamino-phenylchlorphosphin

(2,6-dimethylphenyl)magnesium bromide

Dichlorophenylphosphine

N-methylaniline

Refernces