benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

Base Information

Chemical Name:benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene
CAS No.:616235-15-5
Molecular Formula:C₄₂H₂₄
Molecular Weight:528.653
Hs Code.:

Synonyms:benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

Chemical Property:

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Technology Process of benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

There total 6 articles about benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.5%

: 616235-14-4
3-(1-naphthyl)-7,12-diphenylbenzo[k]fluoranthene

: 616235-15-5
benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

Guidance literature:: 3-(1-naphthyl)-7,12-diphenylbenzo[k]fluoranthene; With boron trifluoride diethyl etherate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; at 20 ℃; for 1h; Inert atmosphere;

With ferrocene; for 1h; Inert atmosphere;

Reference yield:

: 7267-03-0
5-bromoacenaphthylene

: 616235-15-5
benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Reflux

2.1: acetic acid; hydrogen bromide / 12 h / Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; ethanol; water / 12 h / 90 °C

4.1: trifluoroacetic acid; boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

4.2: 1 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron trifluoride diethyl etherate; hydrogen bromide; sodium carbonate; acetic acid; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; water; toluene;

Reference yield:

: C₃₂H₂₁BrO

: 616235-15-5
benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; hydrogen bromide / 12 h / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; ethanol; water / 12 h / 90 °C

3.1: trifluoroacetic acid; boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

3.2: 1 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron trifluoride diethyl etherate; hydrogen bromide; sodium carbonate; acetic acid; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; water; toluene;