cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾

Base Information

Chemical Name:cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾
CAS No.:141272-20-0
Molecular Formula:C₁₇H₁₈CrN₂O₄
Molecular Weight:366.337
Hs Code.:

cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium<sup>(0)</sup>

Synonyms:cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾

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Technology Process of cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾

There total 1 articles about cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1121-22-8,38383-49-2,43148-65-8,46026-77-1,53100-04-2,53152-68-4,53152-69-5
trans-N,N,N′,N′-tetramethylcyclohexane-1,2-diamine

: 27436-93-7
pentacarbonyl(1-methoxybenzylidene)chromium⁽⁰⁾

: 141272-20-0
cis-{trans-2-aminocyclohexylamino(phenyl)carbene-C,N}tetracarbonylchromium⁽⁰⁾

Guidance literature:: In tetrahydrofuran; byproducts: CO; N2 atmosphere; addn. of soln. of org. compd. in THF to soln. of Cr-compd. in THF at 0°C, removal of solvent (vac.), chromy. (silica gel, CH2Cl2, -10°C), dissolution in THF, heating at 65°C for 2 h under N2 flow; removal of solvent (vac.), chromy. (silica gel, -10°C, CH2Cl2/EtOH 95:5), recrystn. from CH2Cl2; elem. anal.;