7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one

Base Information

Chemical Name:7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one
CAS No.:97567-86-7
Molecular Formula:C₁₇H₁₈O₄S
Molecular Weight:318.394
Hs Code.:

Synonyms:7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one

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Technology Process of 7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one

There total 2 articles about 7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 97567-85-6
7,7a-dihydro-7a-methyl-1-(4-methylphenylsulphonyloxy)-6-phenylselenoindan-5(6H)-one

: 97567-86-7
7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one

Guidance literature:: With chloroamine-T; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water;

Reference yield:

: 97567-84-5
7,7a-dihydro-7a-methyl-1-(4-methylphenylsulphonyloxy)indan-5(6H)-one

: 97567-86-7
7a-methyl-1-(4-methylphenylsulphonyloxy)-1,2,3,7a-tetrahydro-5H-inden-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / lithium di-isopropylamide / tetrahydrofuran / 1 h / from -78 deg C to room temp.

2: 95 percent / chloramine-T / benzyltriethylammonium chloride / CH₂Cl₂; H₂O

With chloroamine-T; lithium diisopropyl amide; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; dichloromethane; water;