(3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

Base Information

Chemical Name:(3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide
CAS No.:1026897-61-9
Molecular Formula:C₂₈H₃₅N₆O₄P
Molecular Weight:550.597
Hs Code.:

Synonyms:(3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

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Chemical Property of (3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

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Technology Process of (3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

There total 4 articles about (3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 839677-56-4
2-amino-3-(3-hydroxypropyl)-6,7-diphenyl-4(3H)-pteridinone

: 86030-43-5
N,N-diisopropylmethylphosphonamidic chloride

: 1026897-61-9
(3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1039/b413655a

Reference yield:

: 839677-54-2
5-amino-7-(3-chloropropoxy)furazano[3,4-d]pyrimidine

: 1026897-61-9
(3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol / 2 h / 20 °C

2: 66 mg / Na / methanol / 3 h / Heating

3: 24 percent / diisopropylethylamine / tetrahydrofuran / 1 h / 20 °C

With hydrogen; sodium; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1039/b413655a

Reference yield:

: 6,8,9-triamino-3,4-dihydro-2H-pyrimido[6,1-b][1,3]oxazin-5-ylium; chloride

: 1026897-61-9
(3-(2-amino-3,4-dihydro-4-oxo-6,7-diphenyl-3-pteridynyl)propoxy)diisopropylaminomethoxyphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 216 mg / aq. KOH / methanol / 1.5 h / 40 °C

2: 24 percent / diisopropylethylamine / tetrahydrofuran / 1 h / 20 °C

With potassium hydroxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;
DOI:10.1039/b413655a