(R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

Base Information

Chemical Name:(R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone
CAS No.:226910-57-2
Molecular Formula:C₃₉H₄₆O₅
Molecular Weight:594.791
Hs Code.:

Synonyms:(R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

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Chemical Property of (R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

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Technology Process of (R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

There total 2 articles about (R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 226910-56-1
(R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

: 226910-57-2
(R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; Yield given; Ambient temperature;
DOI:10.1021/ja984250f

Reference yield:

: 226910-55-0
(R)-1-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-(tert-butyl-dimethyl-silanyloxy)-cyclohex-1-enylmethyl]-2,6,6-trimethyl-3-triisopropylsilanyloxy-cyclohex-2-enol

: 226910-57-2
(R)-3-Benzyloxymethyl-5-[(S)-2-(bis-benzyloxy-methyl)-6-hydroxy-cyclohex-1-enylmethyl]-2,4,4-trimethyl-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: benzyl alcohol, 4A molecular sieves, Montmorillonite K₁₀ / CH₂Cl₂ / 1 h / -45 °C

2: TBAF / tetrahydrofuran / Ambient temperature

With 4 A molecular sieve; Montmorillonite K₁₀; tetrabutyl ammonium fluoride; benzyl alcohol; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja984250f