Technology Process of C26H18N2
There total 8 articles about C26H18N2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethyl phosphite;
at 160 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium phosphate; trans-1,2-cyclohexanediamine; copper(l) iodide / 1,4-dioxane / 18 h / 120 °C
2: triethyl phosphite / 20 h / 160 °C
With
potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine; triethyl phosphite;
In
1,4-dioxane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene; ethanol / 90 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
3: potassium phosphate; trans-1,2-cyclohexanediamine; copper(l) iodide / 1,4-dioxane / 18 h / 120 °C
4: triethyl phosphite / 20 h / 160 °C
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; sodium carbonate; trans-1,2-cyclohexanediamine; triethyl phosphite;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; toluene;