24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine

Base Information

• Chemical Name: 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine
• CAS No.: 144231-26-5
• Molecular Formula: C₅₄H₄₂N₆O₄S₂
• Molecular Weight: 903.097

Synonyms:24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine

Chemical Property of 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine

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Technology Process of 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine

There total 3 articles about 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,9-bis(bromomethyl)-4,7-diphenyl-1,10-phenanthroline + 2,9-bis(p-toluenesulfonamidomethyl)-1,10-phenanthroline → 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine (144231-26-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 22 ℃; for 12h;

DOI:10.1248/cpb.40.3334

Reference yield:

2,9-bis(aminomethyl)-1,10-phenanthroline diperchlorate (78831-39-7,144947-65-9) → 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine (144231-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / pyridine / 3 h / 22 °C

2: 91 percent / K₂CO₃ / dimethylformamide / 12 h / 22 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.40.3334

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 24,30-diphenyl-8,19-bis(p-toluenesulfonyl)-1,21:4,6:10,12:15,17-tetraetheno-8,9,19,20-tetrahydro-7H,18H-dibenzo<1,4,7,10,13,16>hexaazacyclooctadecine (144231-26-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / pyridine / 3 h / 22 °C

2: 91 percent / K₂CO₃ / dimethylformamide / 12 h / 22 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.40.3334

upstream raw materials:

2,9-bis(aminomethyl)-1,10-phenanthroline diperchlorate

p-toluenesulfonyl chloride

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