(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

Base Information

Chemical Name:(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol
CAS No.:1613321-18-8
Molecular Formula:C₆₆H₁₀₈FN₉O₁₅
Molecular Weight:1286.63
Hs Code.:

(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

Synonyms:(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

There total 5 articles about (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1613321-17-7
(2S,3S,4R)-2-amino-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)octadecane-1,3,4-triol

: 1613321-02-0
N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyl 4-nitrophenyl carbonate

: 1613321-18-8
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

Guidance literature:: With triethylamine; In pyridine; at 20 ℃; for 32h; Inert atmosphere;

Reference yield:

: 1613321-01-9
N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyl alcohol

: 1613321-18-8
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 41 h / 20 °C / Inert atmosphere

2: triethylamine / pyridine / 32 h / 20 °C / Inert atmosphere

With triethylamine; N-ethyl-N,N-diisopropylamine; In pyridine; N,N-dimethyl-formamide;

Reference yield:

: C₁₁H₁₉N₃O₄

: 1613321-18-8
(2S,3S,4R)-1-O-(α-D-galactopyranosyl)-4-O-(11-(4-fluorophenyl)undecanoyl)-2-(((N-(6-azidohexanoyl)-Val-Cit-4-aminobenzyloxy)carbonyl)amino)octadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; dichloromethane / 2.58 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 41 h / 20 °C / Inert atmosphere

3: triethylamine / pyridine / 32 h / 20 °C / Inert atmosphere

With triethylamine; N-ethyl-N,N-diisopropylamine; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide;