5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione
CAS No.:17242-86-3
Molecular Formula:C₃₀H₂₃FN₂O₉
Molecular Weight:574.519
Hs Code.:

5-fluoro-1-(tri-<i>O</i>-benzoyl-β-<i>D</i>-arabinofuranosyl)-1<i>H</i>-pyrimidine-2,4-dione

Synonyms:5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Suppliers and Price of 5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

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Technology Process of 5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

There total 4 articles about 5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4348-69-0
C₃₀H₂₄N₂O₉

: 17242-86-3
1-(2,3,5-tri-O-benzoyl-β-D-arabinofuranosyl)-5-fluorouracil

Guidance literature:: With fluorine; In acetic acid; at 20 ℃; for 1h;
DOI:10.1007/BF00526095

Reference yield:

: 613-90-1
benzoyl cyanide

: 17242-86-3
5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine / acetonitrile / 2 h / Ambient temperature

2: F₂, 5percent ethanolic triethylamine / acetic acid / 1 h / Ambient temperature

With fluorine; triethylamine; In acetic acid; acetonitrile;
DOI:10.1135/cccc19803217

Reference yield:

: 3083-77-0
araU

: 17242-86-3
5-fluoro-1-(tri-O-benzoyl-β-D-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine / acetonitrile / 2 h / Ambient temperature

2: F₂, 5percent ethanolic triethylamine / acetic acid / 1 h / Ambient temperature

With fluorine; triethylamine; In acetic acid; acetonitrile;
DOI:10.1135/cccc19803217