Technology Process of C19H26O5
There total 4 articles about C19H26O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H26O6;
With
carbon disulfide; sodium hydride; methyl iodide;
In
tetrahydrofuran;
at 0 ℃;
for 2h;
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
toluene;
at 90 ℃;
for 3h;
DOI:10.1007/s11164-012-0702-y
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: mercury(II) diacetate / tetrahydrofuran / 2 h / 20 °C
2.1: oxygen; sodium tetrahydroborate / N,N-dimethyl-formamide / 4 h / 20 °C
3.1: sodium; naphthalene / tetrahydrofuran / 0 °C
4.1: sodium hydride / 3 h / 20 °C
5.1: sodium hydride; carbon disulfide; methyl iodide / tetrahydrofuran / 2 h / 0 °C
5.2: 3 h / 90 °C
With
carbon disulfide; sodium tetrahydroborate; naphthalene; mercury(II) diacetate; oxygen; sodium; sodium hydride; methyl iodide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
5.1: |Barton-McCombie Deoxygenation / 5.2: |Barton-McCombie Deoxygenation;
DOI:10.1007/s11164-012-0702-y
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / 3 h / 20 °C
2.1: sodium hydride; carbon disulfide; methyl iodide / tetrahydrofuran / 2 h / 0 °C
2.2: 3 h / 90 °C
With
carbon disulfide; sodium hydride; methyl iodide;
In
tetrahydrofuran;
2.1: |Barton-McCombie Deoxygenation / 2.2: |Barton-McCombie Deoxygenation;
DOI:10.1007/s11164-012-0702-y
