1-(4-nitrophenyl)-5-phenyl-4,5-dihydrotriazole

Base Information

Chemical Name:1-(4-nitrophenyl)-5-phenyl-4,5-dihydrotriazole
CAS No.:10480-11-2
Molecular Formula:C14H12 N4 O2
Molecular Weight:268.275
Hs Code.:2933990090
Mol file:10480-11-2.mol

Synonyms:D2-1,2,3-Triazoline,1-(p-nitrophenyl)-5-phenyl- (7CI,8CI); NSC 47426

Suppliers and Price of 1-(4-nitrophenyl)-5-phenyl-4,5-dihydrotriazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 1-(4-nitrophenyl)-5-phenyl-4,5-dihydrotriazole

Chemical Property:

Vapor Pressure:4.63E-08mmHg at 25°C
Boiling Point:443.5°Cat760mmHg
Flash Point:222°C
PSA：73.78000
Density:1.35g/cm³
LogP:2.98270

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4-nitrophenyl)-5-phenyl-4,5-dihydrotriazole

There total 4 articles about 1-(4-nitrophenyl)-5-phenyl-4,5-dihydrotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1516-60-5
4-nitrophenyl azide

: 10480-11-2
1-(4-nitrophenyl)-5-phenyl-Δ²-1,2,3-triazoline

Guidance literature:: With choline chloride–urea; at 80 ℃; for 8h; Green chemistry;
DOI:10.1039/c8gc01797b

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 785-81-9,1613-94-1,40339-44-4
4-nitro-N-(phenylmethylene)benzenamine

: 10480-11-2
1-(4-nitrophenyl)-5-phenyl-Δ²-1,2,3-triazoline

Guidance literature:: With water; In 1,4-dioxane; at 20 ℃;
DOI:10.1002/ps.2780420407

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 10480-11-2
1-(4-nitrophenyl)-5-phenyl-Δ²-1,2,3-triazoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C

1.2: 0 - 20 °C

2.1: choline chloride–urea / 8 h / 80 °C / Green chemistry

With hydrogenchloride; choline chloride–urea; sodium nitrite; In water;
DOI:10.1039/c8gc01797b