(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

Base Information

Chemical Name:(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide
CAS No.:870196-12-6
Molecular Formula:C₂₄H₂₂N₄O₂
Molecular Weight:398.464
Hs Code.:

Synonyms:(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

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Chemical Property of (2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

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Technology Process of (2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

There total 1 articles about (2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 700-63-0,6485-52-5,6485-67-2,58429-87-1
(R)-phenylglycine amide

: 623-27-8
terephthalaldehyde,

: 870196-12-6
(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1002/chem.200500440

Reference yield: 99.0%

: 870196-12-6
(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

: 106-95-6
allyl bromide

: 870196-14-8
(2R)-2-({(1R)-1-[4-((1R)-1-{[(1R)-2-amino-2-oxo-1-phenylethyl]amino}-3-butenyl)phenyl]-3-butenyl}amino)-2-phenylethanamide

Guidance literature:: allyl bromide; With zinc; In tetrahydrofuran;

(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/chem.200500440

Reference yield:

: 870196-12-6
(2R)-2-({(E)-[4-({[(1R)-2-amino-2-oxo-1-phenylethyl]imino}methyl)phenyl]methylidene}amino)-2-phenylethanamide

: 1-{4-[(1R)-1-aminobutyl]phenyl}-1-butylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: Zn / tetrahydrofuran

1.2: 99 percent / tetrahydrofuran / 0 - 20 °C

2.1: 74 percent / H₂; aq. AcOH / Pd/C / propan-2-ol / 120 h / 20 °C / ambient pressure

With hydrogen; acetic acid; zinc; palladium on activated charcoal; In tetrahydrofuran; isopropyl alcohol;
DOI:10.1002/chem.200500440