C₂₉H₄₄N₂O₃

Base Information

Chemical Name:C₂₉H₄₄N₂O₃
CAS No.:1220904-27-7
Molecular Formula:C₂₉H₄₄N₂O₃
Molecular Weight:468.68
Hs Code.:

C<sub>29</sub>H<sub>44</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₉H₄₄N₂O₃

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Chemical Property of C₂₉H₄₄N₂O₃

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Technology Process of C₂₉H₄₄N₂O₃

There total 8 articles about C₂₉H₄₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1220904-26-6
C₂₉H₄₆N₂O₃

: 1220904-27-7
C₂₉H₄₄N₂O₃

Guidance literature:: C₂₉H₄₆N₂O₃; With tert-butylhypochlorite; In dichloromethane; for 0.75h;

With triethylamine; In dichloromethane; for 0.75h;

Reference yield:

: 70240-29-8
4-(isopropyloxycarbonyl)benzaldehyde

: 1220904-27-7
C₂₉H₄₄N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / dichloromethane / 30 h / 42 °C

2.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

2.2: 2 h / -78 - 20 °C

2.3: 0 °C

3.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16.25 h / 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 4 h

6.1: triethylamine / isopropyl alcohol / 24 h / Reflux; Molecular sieve; Inert atmosphere

7.1: tert-butylhypochlorite / dichloromethane / 0.75 h

7.2: 0.75 h

With hydrogenchloride; methanol; tert-butylhypochlorite; iodine; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1220904-27-7
C₂₉H₄₄N₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 64 h / 70 °C

2.1: caesium carbonate / dichloromethane / 30 h / 42 °C

3.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

3.2: 2 h / -78 - 20 °C

3.3: 0 °C

4.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16.25 h / 0 - 20 °C

6.1: trifluoroacetic acid / dichloromethane / 4 h

7.1: triethylamine / isopropyl alcohol / 24 h / Reflux; Molecular sieve; Inert atmosphere

8.1: tert-butylhypochlorite / dichloromethane / 0.75 h

8.2: 0.75 h

With hydrogenchloride; methanol; tert-butylhypochlorite; iodine; potassium carbonate; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;