C₂₆H₃₆O₄

Base Information

• Chemical Name: C₂₆H₃₆O₄
• CAS No.: 1267490-90-3
• Molecular Formula: C₂₆H₃₆O₄
• Molecular Weight: 412.569
• Mol file: 1267490-90-3.mol

Synonyms:C₂₆H₃₆O₄

Chemical Property of C₂₆H₃₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₆O₄

There total 3 articles about C₂₆H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

C26H38O4 (1267490-83-4) → C26H36O4 (1267490-90-3)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 ℃; for 1.5h; Molecular sieve;

DOI:10.1002/ejoc.201001104

Reference yield:

C28H40O5 → C26H36O4 (1267490-90-3)

Guidance literature:

Multi-step reaction with 3 steps

1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / -78 - -40 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.5 h / 0 °C / Molecular sieve

With lithium aluminium tetrahydride; dimethyl sulfoxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejoc.201001104

Reference yield:

C28H38O5 (1267490-75-4) → C26H36O4 (1267490-90-3)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - -40 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.5 h / 0 °C / Molecular sieve

With lithium aluminium tetrahydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejoc.201001104

upstream raw materials:

C₂₈H₃₈O₅

C₂₆H₃₈O₄