dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

Base Information

Chemical Name:dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate
CAS No.:78176-09-7
Molecular Formula:CF₃O₃S*C₁₇H₂₂OP
Molecular Weight:422.405
Hs Code.:

Synonyms:dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

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Chemical Property of dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

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Technology Process of dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

There total 6 articles about dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1493-13-6
trifluorormethanesulfonic acid

: 78176-02-0
1-phenyl-1,1,3,3-tetramethyl-3H-2,1-benzoxaphosphole

: 78176-09-7
dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

Guidance literature:: In diethyl ether;
DOI:10.1021/ja00400a037

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 78176-09-7
dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: CH₃MgBr, Mg / tetrahydrofuran; diethyl ether / 1.) reflux, 3 h, 2.) room temperature, 18 h

2: 67 percent / diethyl ether / 24 h

3: 2.) aq. NH₄I / 1.) THF, ether, room temperature, 2 h, 2.) 20 min.

4: 100 percent / sodium hydride / diethyl ether / 6 h / Ambient temperature

5: 81 percent / diethyl ether

With ammonium iodide; methylmagnesium bromide; sodium hydride; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00400a037

Reference yield:

: 1-phenyl-1,3,3-trimethyl-3H-2,1-benzoxaphospholium iodide

: 78176-09-7
dimethylphenyl-(2-(1-methyl-1-hydroxyethyl)phenyl)phosphonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) aq. NH₄I / 1.) THF, ether, room temperature, 2 h, 2.) 20 min.

2: 100 percent / sodium hydride / diethyl ether / 6 h / Ambient temperature

3: 81 percent / diethyl ether

With ammonium iodide; sodium hydride; In diethyl ether;
DOI:10.1021/ja00400a037