(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester

Base Information

Chemical Name:(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester
CAS No.:201815-24-9
Molecular Formula:C₁₁H₁₆O₅
Molecular Weight:228.245
Hs Code.:

Synonyms:(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester

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Technology Process of (1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester

There total 2 articles about (1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 201815-24-9
(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester

Guidance literature:: In tetrahydrofuran; at -30 ℃; for 144h;

Reference yield:

: 6118-51-0
exo-3,6-epoxy-1,2,3,6-tetrahydrophthalic anhydride

: 201815-24-9
(1R,2S,3R,4S)-7-Oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid monoisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd / ethyl acetate

2: diethyl ether / 144 h / -30 °C

With hydrogen; palladium; In diethyl ether; ethyl acetate;
DOI:10.1021/jo971731t