C₈H₉BrClNO₂

Base Information

Chemical Name:C₈H₉BrClNO₂
CAS No.:1009094-09-0
Molecular Formula:C₈H₉BrClNO₂
Molecular Weight:266.522
Hs Code.:

C<sub>8</sub>H<sub>9</sub>BrClNO<sub>2</sub>

Synonyms:C₈H₉BrClNO₂

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Chemical Property of C₈H₉BrClNO₂

Chemical Property:

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Technology Process of C₈H₉BrClNO₂

There total 5 articles about C₈H₉BrClNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈H₇BrClNO₂

: 1009094-09-0
C₈H₉BrClNO₂

Guidance literature:: C₈H₇BrClNO₂; With hydrogenchloride; sodium cyanoborohydride; methyl red; In tetrahydrofuran; methanol; water; for 12h; pH=3;

With sodium hydroxide; In tetrahydrofuran; methanol; water; pH=9;

Reference yield:

: 174913-09-8
2-bromo-5-chloroanisole

: 1009094-09-0
C₈H₉BrClNO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron tribromide / dichloromethane / 12.33 h / -40 - 20 °C

2.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.25 h / 160 °C / Microwave irradiation

2.2: 2 h / Heating / reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

3.2: 20 °C

4.1: sodium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 1 h / 20 °C / pH 9

5.1: hydrogenchloride; sodium cyanoborohydride; methyl red / tetrahydrofuran; methanol; water / 12 h / pH 3

5.2: pH 9

With hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; boron tribromide; sodium cyanoborohydride; potassium carbonate; triethylamine; methyl red; magnesium chloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1009094-06-7
3-bromo-6-chloro-2-hydroxybenzaldehyde

: 1009094-09-0
C₈H₉BrClNO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 20 °C

2.1: sodium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 1 h / 20 °C / pH 9

3.1: hydrogenchloride; sodium cyanoborohydride; methyl red / tetrahydrofuran; methanol; water / 12 h / pH 3

3.2: pH 9

With hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; sodium cyanoborohydride; potassium carbonate; methyl red; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;