Ethyl diazoacetate

Base Information Edit

Chemical Name:Ethyl diazoacetate
CAS No.:623-73-4
Molecular Formula:C4H6N2O2
Molecular Weight:114.104
Hs Code.:29270000
European Community (EC) Number:210-810-8
NSC Number:79147
UNII:N84B835FMR
DSSTox Substance ID:DTXSID10878732
Nikkaji Number:J2.294.246H,J25.573D,J3.230.208D,J3.230.209B
Wikipedia:Ethyl_diazoacetate
Wikidata:Q3026455
ChEMBL ID:CHEMBL4212182
Mol file:623-73-4.mol

Synonyms:diazoacetic ester;ethyl diazoacetate

Suppliers and Price of Ethyl diazoacetate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
EthylDiazoacetate(>90%)
20g
$ 80.00

Sigma-Aldrich
Ethyl diazoacetate contains ≥13 wt. % dichloromethane
1kg
$ 1330.00

Sigma-Aldrich
Ethyl diazoacetate contains ≥13 wt. % dichloromethane
20g
$ 78.30

Sigma-Aldrich
Ethyl diazoacetate contains ≥13 wt. % dichloromethane
5g
$ 26.70

Sigma-Aldrich
Ethyl diazoacetate contains ≥13 wt. % dichloromethane
100g
$ 244.00

Medical Isotopes, Inc.
Ethyl diazoacetate
10 g
$ 620.00

Matrix Scientific
Ethyl 2-diazoacetate (diluted with ~10% dichloromethane wt/wt)97%
250g
$ 864.00

Matrix Scientific
Ethyl 2-diazoacetate (diluted with ~10% dichloromethane wt/wt)97%
500g
$ 1440.00

American Custom Chemicals Corporation
ETHYL DIAZOACETATE 95.00%
100G
$ 2823.28

American Custom Chemicals Corporation
ETHYL DIAZOACETATE 95.00%
20G
$ 1148.53

Total 39 raw suppliers

Chemical Property of Ethyl diazoacetate Edit

Chemical Property:

Appearance/Colour:colourless liquid
Melting Point:-22 °C
Refractive Index:n20/D 1.46(lit.)
Boiling Point:140-141 °C (720 mmHg)
Flash Point:46 °C
PSA：63.69000
Density:1.085 g/cm³
LogP:-0.06884
Storage Temp.:2-8°C
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:114.042927438
Heavy Atom Count:8
Complexity:126

Purity/Quality:

99% ^*data from raw suppliers

EthylDiazoacetate(>90%) ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xn
Hazard Codes:Xn,F
Statements: 5-10-22-40-67-65-48/20-38-11-63
Safety Statements: 36/37-62-16

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Chemical Classes:Nitrogen Compounds -> Other Nitrogen Compounds
Canonical SMILES:CCOC(=O)C=[N+]=[N-]
Uses Reagent for ruthenium-catalyzed asymmetric cyclopropanation of alkenes.1

Technology Process of Ethyl diazoacetate

There total 51 articles about Ethyl diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.4%

: 623-33-6
glycine ethyl ester hydrochloride

: 623-73-4
diazoacetic acid ethyl ester

Guidance literature:: With hydrogenchloride; sodium sulfite; sodium nitrite; In dichloromethane; water; at 3 ℃; for 4h; pH=4.3; Solvent; Temperature; Reagent/catalyst; pH-value; Large scale;