S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

Base Information

Chemical Name:S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine
CAS No.:119835-94-8
Molecular Formula:C₂₄H₂₃N₃O₇
Molecular Weight:465.463
Hs Code.:

Synonyms:S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

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Technology Process of S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

There total 5 articles about S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119835-93-7
S-(-)-5-(3'-benzyloxybenzyl)-1-<(1'-phtalimidomethyl-2'-benzyloxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

: 119835-94-8
S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; for 0.5h; under 2280 Torr;
DOI:10.1002/jhet.5570250561

Reference yield:

: 1074-82-4
potassium phtalimide

: 119835-94-8
S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / dimethylformamide / 0.5 h / 120 °C

2: HCl (g) / CH₂Cl₂ / 3 h / 0 °C

3: 75 percent / K₂CO₃ (s) / CH₂Cl₂ / 48 h / Ambient temperature

4: H₂, 6 N HCl / 10percent Pd/C / methanol; CH₂Cl₂ / 0.5 h / 2280 Torr

With hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570250561

Reference yield:

: 119835-78-8
2-((R)-3-Benzyloxy-2-chloromethoxy-propyl)-isoindole-1,3-dione

: 119835-94-8
S-(-)-5-(3'-hydroxybenzyl)-1-<(1'-phtalimidomethyl-2'-hydroxyethoxy)methyl>-2-oxo-4-methoxypyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / K₂CO₃ (s) / CH₂Cl₂ / 48 h / Ambient temperature

2: H₂, 6 N HCl / 10percent Pd/C / methanol; CH₂Cl₂ / 0.5 h / 2280 Torr

With hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1002/jhet.5570250561