2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine

Base Information

Chemical Name:2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine
CAS No.:1380391-54-7
Molecular Formula:C₂₉H₂₈Cl₅N₅O₆
Molecular Weight:719.836
Hs Code.:

Synonyms:2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine

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Chemical Property of 2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine

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Technology Process of 2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine

There total 1 articles about 2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380391-55-8
2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-vinyl-β-D-ribofuranosyl]-9H-purine

: 1380391-54-7
2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine

Guidance literature:: 2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-vinyl-β-D-ribofuranosyl]-9H-purine; With 4-methylmorpholine N-oxide; osmium(VIII) oxide; In 1,4-dioxane; water; for 14h;

With sodium periodate; In dichloromethane; for 12h;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 4h;

Reference yield:

: 1380391-54-7
2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine

: 1380391-53-6
2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-fluoromethyl-β-D-ribofuranosyl]-9H-purine

Guidance literature:: 2-(isobutyrylamino)-6-chloro-9-[3,5-bis-O-(2,4-dichlorobenzyl)-2-C-hydroxymethyl-β-D-ribofuranosyl]-9H-purine; With dmap; trifluoromethylsulfonic anhydride; triethylamine; In dichloromethane; at -10 ℃; for 1h;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 4h;