(1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate

Base Information

Chemical Name:(1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate
CAS No.:906548-45-6
Molecular Formula:C₁₀H₁₆O₂*C₁₂H₁₉NO₂S
Molecular Weight:409.59
Hs Code.:

Synonyms:(1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate

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Chemical Property of (1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate

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Technology Process of (1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate

There total 1 articles about (1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 906548-44-5
(1S,2S)-(+)-2-(dimethylamino)-1-[4-(methylthio)phenyl]propane-1,3-diol

: trans-chrysanthemic acid

: C₁₀H₁₆O₂*C₁₂H₁₉NO₂S

: 906548-45-6
(1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate

Guidance literature:: In di-isopropyl ether; for 0.5h; Purification / work up; Resolution of racemate; Heating / reflux;

Reference yield:

: 906548-45-6
(1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate

: 906548-44-5
(1S,2S)-(+)-2-(dimethylamino)-1-[4-(methylthio)phenyl]propane-1,3-diol

: 2259-14-5
(1S,3S)-trans-chrysanthemic acid

Guidance literature:: (1S,2S)-(+)-1,3-dihydroxy-N,N-dimethyl-1-[4-(methylthio)phenyl]propan-2-amino (1S,3S)-(-)-2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropanecarboxylate; With hydrogenchloride; In water;

With sodium hydroxide; In water; pH=10; Product distribution / selectivity;