(2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

Base Information

Chemical Name:(2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal
CAS No.:1307901-00-3
Molecular Formula:C₂₀H₂₅FN₂O₅S₂
Molecular Weight:456.559
Hs Code.:

Synonyms:(2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

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Chemical Property of (2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

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Technology Process of (2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

There total 1 articles about (2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 929049-05-8
(2S,4R)-N-[4-hydroxy-5-methoxy-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

: 106-96-7
propargyl bromide

: 1307901-00-3
(2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

Guidance literature:: With potassium carbonate; In acetone; Reflux;
DOI:10.1016/j.bmc.2011.03.015

Reference yield: 85.0%

: 1307901-00-3
(2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

: 1307900-64-6
3-(5-azidopentyloxy)-17-hydroxy-1,3,5⁽¹⁰⁾-estratriene

: 1307901-09-2
C₄₃H₅₈FN₅O₇S₂

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2011.03.015

Reference yield: 82.0%

: 1307900-63-5
3-(3-azidopropyloxy)-17-hydroxy-1,3,5⁽¹⁰⁾-estratriene

: 1307901-00-3
(2S,4R)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-4-fluoropyrrolidine-2-carboxaldehyde diethyl-dithioacetal

: 1307901-08-1
C₄₁H₅₄FN₅O₇S₂

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2011.03.015