N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine

Base Information

• Chemical Name: N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine
• CAS No.: 1146622-74-3
• Molecular Formula: C₃₉H₄₁N₅O₄
• Molecular Weight: 643.786

Synonyms:N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine

Chemical Property of N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine

Chemical Property:

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Technology Process of N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine

There total 1 articles about N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N1-benzyloxycarbonyl-N2-(tert-butoxycarbonyl)-N3-trifluoromethanesulfonylguanidine (216584-27-9) + 4-(3-aminopropyl)-1-(triphenylmethyl)-imidazole (195053-89-5) → N1-(benzyloxycarbonyl)-N2-(tert-butoxycarbonyl)-N3-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine (1146622-74-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/jm9000693

Reference yield: 93.0%

N1-(benzyloxycarbonyl)-N2-(tert-butoxycarbonyl)-N3-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine (1146622-74-3) → N1-(tert-butoxycarbonyl)-N2-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine (1146622-60-7)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h;

DOI:10.1021/jm9000693

upstream raw materials:

N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine

4-(3-aminopropyl)-1-(triphenylmethyl)-imidazole

Downstream raw materials:

N₁-(tert-butoxycarbonyl)-N₂-[3-(1-trityl-1H-imidazol-4-yl)propyl]guanidine

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