naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

Base Information

Chemical Name:naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester
CAS No.:1242185-46-1
Molecular Formula:C₃₂H₂₈N₄O₄
Molecular Weight:532.599
Hs Code.:

Synonyms:naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

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Chemical Property of naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

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Technology Process of naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

There total 1 articles about naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

: 1012860-26-2
N-allyl-2-[(3R)-3-(hydroxymethyl)-2-oxo-5-phenyl-2,3-dihydro-1H-1,4-benzodiazepin-1-yl]acetamide

: 86-84-0
1-Naphthyl isocyanate

: 1242185-46-1
naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.06.010

Reference yield: 74.0%

: 1242185-46-1
naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

: 140-88-5,9003-32-1
ethyl acrylate

: 1402828-81-2
C₃₅H₃₂N₄O₆

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 100 ℃; for 1h; Microwave irradiation;
DOI:10.1002/cmdc.201200274

Reference yield: 72.7%

: 106-63-8,26335-74-0
isobutyl acrylate

: 1242185-46-1
naphthalen-2-yl-carbamic acid 1-allylcarbamoylmethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl-methyl ester

: 1402828-82-3
C₃₇H₃₆N₄O₆

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 100 ℃; for 1h; Microwave irradiation;
DOI:10.1002/cmdc.201200274