Technology Process of C23H26N2O4*ClH
There total 5 articles about C23H26N2O4*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: acetyl chloride / Reflux
2: sodium hydrogencarbonate / methanol; water / 0 - 20 °C
3: pyridine / 3 h / 0 °C
4: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / acetonitrile; hexane / 12 h / 60 °C / Inert atmosphere
5: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
With
pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; sodium hydrogencarbonate; triethylamine; acetyl chloride;
In
1,4-dioxane; methanol; hexane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / methanol; water / 0 - 20 °C
2: pyridine / 3 h / 0 °C
3: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / acetonitrile; hexane / 12 h / 60 °C / Inert atmosphere
4: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
With
pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; sodium hydrogencarbonate; triethylamine;
In
1,4-dioxane; methanol; hexane; water; acetonitrile;