N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

Base Information

Chemical Name:N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide
CAS No.:1345042-45-6
Molecular Formula:C₂₂H₂₁N₃O₃
Molecular Weight:375.427
Hs Code.:

Synonyms:N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

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Chemical Property of N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

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Technology Process of N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

There total 7 articles about N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₅N₃O₄

: 1345042-45-6
N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In acetone; at 70 ℃; for 40h;
DOI:10.1002/anie.201103597

Reference yield:

: 6973-60-0
1-Methyl-2-pyrrolecarboxylic acid

: 1345042-45-6
N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / N,N-dimethyl-formamide; toluene / 1 h / Inert atmosphere; Reflux

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / acetone / 40 h / 70 °C

With thionyl chloride; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/anie.201103597

Reference yield:

: 1345042-42-3
N-(2-(1,3-dioxolan-2-yl)phenyl)-2-bromoacetamide

: 1345042-45-6
N-benzyl-N-(2-(2-formylphenylamino)-2-oxoethyl)-1-methyl-1H-pyrrole-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 18 h

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / acetone / 40 h / 70 °C

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetone;
DOI:10.1002/anie.201103597