C₂₂H₂₇ClN₄O₆S

Base Information

Chemical Name:C₂₂H₂₇ClN₄O₆S
CAS No.:1159610-60-2
Molecular Formula:C₂₂H₂₇ClN₄O₆S
Molecular Weight:510.999
Hs Code.:

C<sub>22</sub>H<sub>27</sub>ClN<sub>4</sub>O<sub>6</sub>S

Synonyms:C₂₂H₂₇ClN₄O₆S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₇ClN₄O₆S

Chemical Property:

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Technology Process of C₂₂H₂₇ClN₄O₆S

There total 10 articles about C₂₂H₂₇ClN₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24065-33-6
5-Chlorothiophene-2-carboxylic acid

: 1159610-59-9
C₁₇H₂₆N₄O₅

: 1159610-60-2
C₂₂H₂₇ClN₄O₆S

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1159610-60-2
C₂₂H₂₇ClN₄O₆S

Guidance literature:: Multi-step reaction with 10 steps

1: acetonitrile / Reflux

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3: triethylamine / 6 h / Reflux

4: hydrazine / ethanol / 2 h / 20 °C / Reflux

5: sodium carbonate / 1,4-dioxane; water / 4 h / 20 °C

6: hydrogenchloride; zinc / tetrahydrofuran; acetic acid / 2 h / 0 °C

7: isopropyl alcohol / 6 h / Reflux

8: tetrahydrofuran / 12 h

9: hydrazine / ethanol / 2 h / Reflux

10: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 1 h / 0 °C

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine; zinc; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 1965-54-4
N-(2-hydroxyethyl)-4-nitroaniline

: 1159610-60-2
C₂₂H₂₇ClN₄O₆S

Guidance literature:: Multi-step reaction with 9 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: triethylamine / 6 h / Reflux

3: hydrazine / ethanol / 2 h / 20 °C / Reflux

4: sodium carbonate / 1,4-dioxane; water / 4 h / 20 °C

5: hydrogenchloride; zinc / tetrahydrofuran; acetic acid / 2 h / 0 °C

6: isopropyl alcohol / 6 h / Reflux

7: tetrahydrofuran / 12 h

8: hydrazine / ethanol / 2 h / Reflux

9: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 1 h / 0 °C

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; hydrazine; zinc; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;