2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

Base Information

Chemical Name:2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine
CAS No.:672279-32-2
Molecular Formula:C₂₅H₃₅NO₂
Molecular Weight:381.558
Hs Code.:

Synonyms:2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

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Chemical Property of 2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

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Technology Process of 2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

There total 7 articles about 2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₂₅H₃₃NO₂

: 672279-32-2
2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h;
DOI:10.1134/S1070428011010143

Reference yield:

: 23659-45-2
rac-2-isopropyltetrahydropyran-4-one

: 672279-32-2
2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

Guidance literature:: Multi-step reaction with 6 steps

3: potassium hydroxide

4: lithium aluminium tetrahydride / diethyl ether / Cooling

5: benzene / 4 h / Reflux

6: sodium tetrahydroborate / methanol / 1 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; potassium hydroxide; In methanol; diethyl ether; benzene;
DOI:10.1134/S1070428011010143

Reference yield:

: 713114-06-8
[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]acetonitrile

: 672279-32-2
2-[2-isopropyl-4-(p-tolyl)tetrahydro-2H-pyran-4-yl]-N-(4-methoxybenzyl)ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / Cooling

2: benzene / 4 h / Reflux

3: sodium tetrahydroborate / methanol / 1 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; In methanol; diethyl ether; benzene;
DOI:10.1134/S1070428011010143