2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:668438-54-8
Molecular Formula:C₅₂H₆₄BNO₄
Molecular Weight:777.895
Hs Code.:

Synonyms:2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Chemical Property of 2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of 2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 1 articles about 2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 668438-52-6
3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl bromide

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 668438-54-8
2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: 3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl bromide; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 1h; Cooling with acetone-dry ice;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 - 20 ℃; for 20h; Cooling with acetone-dry ice;

Reference yield: 27.0%

: 58530-53-3
2,4-dibromopyridine

: 668438-54-8
2-(3-{3',6'-di[4''-(2'''-ethylhexyloxy)phenyl]carbazolyl}phenyl)-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 4-bromo-2-(3'-{3'',6''-di[4'''-(2''''-ethylhexyloxy)phenyl]carbazolyl}phenyl)pyridine

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 45h; Heating / reflux;