methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

Base Information

Chemical Name:methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate
CAS No.:445255-17-4
Molecular Formula:C₈₂H₁₀₈O₈
Molecular Weight:1221.75
Hs Code.:

Synonyms:methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

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Chemical Property of methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

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Technology Process of methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

There total 5 articles about methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 213680-85-4
1,3-bis{[3,5-bis(tert-butyl)benzyl]oxy}-5-(bromomethyl)benzene

: 445255-17-4
methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 48h; Heating;
DOI:10.1021/ol062793l

Reference yield:

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 445255-17-4
methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran / 4 h / 20 °C

3: 81 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

4: 93 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/ol062793l

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 445255-17-4
methyl 3,5-bis[(3,5-bis{[3,5-bis(tert-butyl)benzyl]oxy}benzyl)oxy]benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran / 4 h / 20 °C

3: 81 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

4: 93 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1021/ol062793l