3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

Base Information

Chemical Name:3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride
CAS No.:1261228-80-1
Molecular Formula:C₁₆H₂₄N₂O₂*ClH
Molecular Weight:312.84
Hs Code.:

Synonyms:3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

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Technology Process of 3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

There total 3 articles about 3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1261228-75-4
3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene

: 1261228-80-1
3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

Guidance literature:: With hydrogenchloride; In benzene;
DOI:10.1007/s11172-010-0192-2

Reference yield:

: 17160-89-3
1-acetylcyclopentanol

: 1261228-80-1
3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 5 h / 40 °C

2: hydrogenchloride / benzene

With hydrogenchloride; sodium methylate; In methanol; benzene;
DOI:10.1007/s11172-010-0192-2

Reference yield:

: 15029-38-6
2-cyano-N-cyclohexylacetamide

: 1261228-80-1
3-(N-cyclohexylcarbamoyl)-2-imino-4-methyl-1-oxaspiro[4.4]non-3-ene hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 5 h / 40 °C

2: hydrogenchloride / benzene

With hydrogenchloride; sodium methylate; In methanol; benzene;
DOI:10.1007/s11172-010-0192-2