2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

Base Information

Chemical Name:2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane
CAS No.:1133292-27-9
Molecular Formula:C₄₈H₅₁FO₄Si
Molecular Weight:739.014
Hs Code.:

Synonyms:2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

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Chemical Property of 2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

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Technology Process of 2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

There total 1 articles about 2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1133292-22-4
4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl bromide

: 1133292-25-7
2,2-dibenzyl-3-(4-methoxybenzyloxy)propan-1-ol

: 1133292-27-9
2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

Guidance literature:: 2,2-dibenzyl-3-(4-methoxybenzyloxy)propan-1-ol; With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.0833333h; Inert atmosphere;

4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyl bromide; In tetrahydrofuran; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jo900026e

Reference yield: 92.0%

: 1133292-27-9
2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

: 1133292-31-5
2,2-dibenzyl-1-(4-hydroxy-3-fluorobenzyloxy)-3-(4-methoxybenzyloxy)propane

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo900026e

Reference yield: 89.0%

: 1133292-27-9
2,2-dibenzyl-1-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]-3-(4-methoxybenzyloxy)propane

: 1133292-29-1
2,2-dibenzyl-3-[4-(tert-butyldiphenylsilyloxy)-3-fluorobenzyloxy]propan-1-ol

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo900026e