tert-butyl amino>ethanoate

Base Information

Chemical Name:tert-butyl amino>ethanoate
CAS No.:123642-59-1
Molecular Formula:C₁₆H₂₄N₂O₆
Molecular Weight:340.376
Hs Code.:

tert-butyl <N-<1-(4',5'-dimethoxy-2'-nitrophenyl)ethyl>amino>ethanoate

Synonyms:tert-butyl amino>ethanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl amino>ethanoate

Chemical Property:

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Technology Process of tert-butyl amino>ethanoate

There total 3 articles about tert-butyl amino>ethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 107-59-5
tert-Butyl chloroacetate

: 123642-58-0
<1-(4',5'-dimethoxy-2'-nitrophenyl)ethyl>amine

: 123642-59-1
tert-butyl amino>ethanoate

Guidance literature:: With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In acetonitrile; at 60 ℃; for 15h;
DOI:10.1021/jo00292a038

Reference yield:

: 4101-32-0
4',5'-dimethoxy-2'-nitroacetophenone

: 123642-59-1
tert-butyl amino>ethanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 23.6 percent / NH₄OAc, NaBH₃CN / methanol / 1) r.t, 4 days 2) 60 deg C, 24h

2: 39 percent / N,N,N',N'-tetramethyl-1,8-napthalenediamine / acetonitrile / 15 h / 60 °C

With ammonium acetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium cyanoborohydride; In methanol; acetonitrile;
DOI:10.1021/jo00292a038

Reference yield:

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 123642-59-1
tert-butyl amino>ethanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / HNO₃ conc. / 1 h / 18 - 22 °C

2: 23.6 percent / NH₄OAc, NaBH₃CN / methanol / 1) r.t, 4 days 2) 60 deg C, 24h

3: 39 percent / N,N,N',N'-tetramethyl-1,8-napthalenediamine / acetonitrile / 15 h / 60 °C

With ammonium acetate; nitric acid; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; sodium cyanoborohydride; In methanol; acetonitrile;
DOI:10.1021/jo00292a038